NMR analysis was performed on a Bruker AMX-500 spectrometer. The sample was deuterium-exchanged by lyophilization from D2O and dissolved in 0.5 mL DMSO-d6/D2O 982. The 1H-NMR 1D spectrum was obtained at 308(K (35(C) at 500 MHz, using presaturation of the residual HOD signal. Chemical shifts were measured relative to the residual protonated DMSO-d6 centered at 2.503 ppm (measured relative to TMS=0.0ppm).

Agency
National Institute of Health (NIH)
Institute
National Center for Research Resources (NCRR)
Type
Biotechnology Resource Grants (P41)
Project #
5P41RR005351-13
Application #
6493694
Study Section
Project Start
2001-08-01
Project End
2002-07-31
Budget Start
Budget End
Support Year
13
Fiscal Year
2001
Total Cost
$288,015
Indirect Cost
Name
University of Georgia
Department
Type
DUNS #
City
Athens
State
GA
Country
United States
Zip Code
30602
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