Biosynthetic oligosaccharide samples were submitted for confirmation of their structure and generation of standard 1H- and 13C-NMR spectra for company files. The samples were exchanged repeatedly in D2O and subjected to 1H- and 13C-NMR analysis at 500 and 125.77 MHz, respectively. 1-D spectra were acquired on a Bruker AMX-500 NMR instrument at 25(C. Chemical shifts were assigned relative to acetone, and the oligosaccharide sequences, anomeric configurations, and linkages were assigned by comparison with previously published spectra of synthetic oligosaccharides of identical structure.

Agency
National Institute of Health (NIH)
Institute
National Center for Research Resources (NCRR)
Type
Biotechnology Resource Grants (P41)
Project #
5P41RR005351-10
Application #
6122220
Study Section
Project Start
1998-09-30
Project End
1999-07-31
Budget Start
1997-10-01
Budget End
1998-09-30
Support Year
10
Fiscal Year
1998
Total Cost
Indirect Cost
Name
University of Georgia
Department
Type
DUNS #
City
Athens
State
GA
Country
United States
Zip Code
30602
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