The intent of this project is to establish the fracture characteristics of a hybrid composite in the ratio of 1/9 microfill to small particle filler and the corresponding unfilled Bis-GMA/ TEDMA resin. This approach is based on the experimental and clinical results which demonstrate that dental composite restorative materials when subject to aging in the oral cavity and the forces of mastication can fail in fatigue due to the effects of stress corrosion, microcracking and particle separation. The experimental procedures consist of fatiguing notched specimens n distilled water at 37oC under fatigue flexure (three point loading). The fracture process will be observed by means of a long range optical microscope. Fracture surface characterization and damage analysis will be carried out on the fractured specimens using principals of quantitative stereology which are widely employed in materials science. The analytical study is aimed at modeling the observed phenomena using principles of fracture mechanics with the theory of statistics incorporated to analyze the scatter of the fracture data. The work of this project attempts to directly link the microscopic measures of fracture initiation and propagation to microstructural variables and ultimately to processing parameters. This knowledge can be used to design better materials as well as longer lasting and more economical dental composites. Alternatively, this approach will provide greater understanding of the fracture behavior of dental composites and the relationship to microstructure under mechanical and environmental loadings. Furthermore, the results of this work will allow us to test the validity and reliability of the techniques employed in engineering to predict the life-time and fracture toughness of dental composites.

Agency
National Institute of Health (NIH)
Institute
National Institute of Dental & Craniofacial Research (NIDCR)
Type
Research Project (R01)
Project #
5R01DE007979-02
Application #
3221750
Study Section
Oral Biology and Medicine Subcommittee 1 (OBM)
Project Start
1990-07-01
Project End
1993-06-30
Budget Start
1991-07-01
Budget End
1992-06-30
Support Year
2
Fiscal Year
1991
Total Cost
Indirect Cost
Name
University of Illinois at Chicago
Department
Type
Schools of Dentistry
DUNS #
121911077
City
Chicago
State
IL
Country
United States
Zip Code
60612
Patki, Amol S; Vural, Murat; Gosz, Mike (2011) Confined compression of dental composites for Class I restorations. J Compos Mater 45:1863-1872
Lin, Lihong; Drummond, James L (2010) Cyclic loading of notched dental composite specimens. Dent Mater 26:207-14
Akhmetov, Artem; Moore, Jerry F; Gasper, Gerald L et al. (2010) Laser desorption postionization for imaging MS of biological material. J Mass Spectrom 45:137-45
Aydin Sevinc, Berdan; Hanley, Luke (2010) Antibacterial activity of dental composites containing zinc oxide nanoparticles. J Biomed Mater Res B Appl Biomater 94:22-31
Drummond, James L; Lin, Lihong; Al-Turki, Lulwa A et al. (2009) Fatigue behaviour of dental composite materials. J Dent 37:321-30
Kotche, Miiri; Drummond, James L; Sun, Kang et al. (2009) Multiaxial analysis of dental composite materials. J Biomed Mater Res B Appl Biomater 88:412-8
Drummond, J L (2008) Degradation, fatigue, and failure of resin dental composite materials. J Dent Res 87:710-9
Koin, P J; Kilislioglu, A; Zhou, M et al. (2008) Analysis of the degradation of a model dental composite. J Dent Res 87:661-5
Zhou, Manshui; Wu, Chunping; Akhmetov, Artem et al. (2007) 7.87 eV laser desorption postionization mass spectrometry of adsorbed and covalently bound bisphenol A diglycidyl methacrylate. J Am Soc Mass Spectrom 18:1097-108
Al-Turki, Lulwa I; Drummond, James L; Agojci, Majlinda et al. (2007) Contact versus flexure fatigue of a fiber-filled composite. Dent Mater 23:648-53

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